Drilling Fluid

Testing Gilsonite in the Mud Laboratory

· 1 min read · Sun Gilsonite Technical Team

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Testing Gilsonite in the Mud Laboratory – 25 kg kraft paper bags of sulphonated asphalt

Before a field trial, laboratory testing confirms that a gilsonite grade suits your fluid and well conditions.

Basic tests

  • Rheology (API RP 13B) before and after addition
  • API fluid loss at room temperature
  • HPHT fluid loss at bottom-hole temperature
  • Hot rolling to simulate circulation

Shale tests

  • Linear swell tests
  • Shale dispersion (cuttings recovery)
  • Pore pressure transmission tests
25 kg kraft paper bags of sulphonated asphalt – drilling fluid application

Particle size and softening point

Confirm that the grade’s particle size distribution and softening point match the specification.

Interpreting results

A good gilsonite treatment lowers HPHT fluid loss, gives thin firm filter cakes and improves shale recovery, without unacceptable rheology changes.

Example test matrix

Sample Gilsonite Test temperature
Base mud 0 lb/bbl BHT
A 4 lb/bbl, grade 1 BHT
B 4 lb/bbl, grade 2 BHT
C 6 lb/bbl, best grade BHT

Reporting

Report rheology, API and HPHT filtrate, cake thickness and shale results in one table to compare options easily.

Sample request

Sun Gilsonite can send samples of drilling grade gilsonite and sulphonated asphalt for testing. See HPHT fluid loss control.

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Data sheet

Drilling Fluid Grade Gilsonite

Data sheet – Drilling Fluid Grade Gilsonite
PropertyTypical valueTest method
AppearanceBlack, shiny powderVisual
Softening point (R&B)160 – 220 °C (grades)ASTM D36
Ash content3 – 8 %ASTM D3174
Solubility in TCE95 – 99 %ASTM D2042
Specific gravity @ 25°C1.04 – 1.06ASTM D70
Moisture, max1 %ASTM D95
Particle size75 – 200 µmSieve
Typical dosage2 – 8 lb/bbl
Packing25 kg (50 lb) bags palletized; 1 MT jumbo bags.

Typical values. The final specification is confirmed in the COA of each shipment.

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